Journals Information
Universal Journal of Chemistry(CEASE PUBLICATION) Vol. 2(1), pp. 1 - 5
DOI: 10.13189/ujc.2014.020101
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Mercury Determination by New Asymmetric Triazene Ligand, 1-(2-Ethoxyphenyl)-3-(4-Nitrophenyl)Triazene (ENT) ) with Partial Least-Squares Calibration Method (PLS) Method
Salameh Azimi 1,*, Mohammadreza Sadeghi Moghaddam 2
1 Faculty of Industrial and Mechanical Engineering, Qazvin Branch, Islamic Azad University, Qazvin, Iran
2 Department of urban planning, Qazvin Branch, Islamic Azad University, Qazvin, Iran
ABSTRACT
Synthesis, characterization, spectrophotometric studies of three mercury (II) complexes of 1-(2-ethoxyphenyl)-3-(4-nitrophenyl) triazene (ENT) are reported in this article and it was characterized by means of NMR, FT-IR, UV spectroscopy and CHN analysis, then determination of Hg(II) was performed by spectrophotometric determination using chemo metric techniques and new triazen ligand which was prepared by us. The calibration graphs of individual components were linear in the ranges of 1 -5.25 mg鈥-1. The root means square errors of prediction (RMSEP) were 4.4 褏10-3 The proposed method are simple, fast, inexpensive and do not need to any separation or preparation method.
KEYWORDS
Synthesis, Triazen Ligand, Spectrophotometric Determinatio Chemo Metric Techniques, Mercury
Cite This Paper in IEEE or APA Citation Styles
(a). IEEE Format:
[1] Salameh Azimi , Mohammadreza Sadeghi Moghaddam , "Mercury Determination by New Asymmetric Triazene Ligand, 1-(2-Ethoxyphenyl)-3-(4-Nitrophenyl)Triazene (ENT) ) with Partial Least-Squares Calibration Method (PLS) Method," Universal Journal of Chemistry(CEASE PUBLICATION), Vol. 2, No. 1, pp. 1 - 5, 2014. DOI: 10.13189/ujc.2014.020101.
(b). APA Format:
Salameh Azimi , Mohammadreza Sadeghi Moghaddam (2014). Mercury Determination by New Asymmetric Triazene Ligand, 1-(2-Ethoxyphenyl)-3-(4-Nitrophenyl)Triazene (ENT) ) with Partial Least-Squares Calibration Method (PLS) Method. Universal Journal of Chemistry(CEASE PUBLICATION), 2(1), 1 - 5. DOI: 10.13189/ujc.2014.020101.