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Universal Journal of Materials Science Vol. 2(5), pp. 83 - 89
DOI: 10.13189/ujms.2014.020501
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Ti₃SiC₂ MAX Phase Synthesis by Plasma Basis Method

Badis Bendjemil ^1,2,*, Faming Zhang ^3,4
1 LASEA, Department of Chemistry, University of Badji-Mokhtar, 23000 Annaba, Algeria
² University of 8 Mai 1945 Guelma, 24000 Guelma, Algeria
³ Physics of new Materials, Institute of Physics, University of Rostock, 18055 Rostock, Germany
⁴ School of Materials Science and Engineering, Southeast University, 211189 Nanjing, China

ABSTRACT

The polycrystalline dense Ti₃SiC₂ based ceramic have been prepared by several techniques. The effects on the addition of TiC or SiC are also studied. Ti₃SiC₂ has an unusual combination of electrical, thermal and mechanical extraordinary properties. It has furthermore damage tolerant and oxidation resistance. In this work we have produced Ti₃SiC₂ by electro-thermal explosion chemical reaction started with high current density (680 amperes) followed by uniaxial pressure. The microstructures of the materials were studied using XRD, SEM and EDX. The surface of Ti₃SiC₂ was studied by means of X-ray photoelectron spectroscopy (XPS). High resolution C_1s, Si_2p, Ti_2p, Ti_3s core level spectra are inspected in terms of electronic structure. Valence band spectra will be performed to confirm the validity of the theoretical calculations.

KEYWORDS
Ti₃SiC₂ Based Ceramic, Intermetallic, Bicarbide, Electro-thermal Explosion Reaction (ETE), Core Level Excitation, XPS

Cite This Paper in IEEE or APA Citation Styles
(a). IEEE Format:
[1] Badis Bendjemil , Faming Zhang , "Ti₃SiC₂ MAX Phase Synthesis by Plasma Basis Method," Universal Journal of Materials Science, Vol. 2, No. 5, pp. 83 - 89, 2014. DOI: 10.13189/ujms.2014.020501.

(b). APA Format:
Badis Bendjemil , Faming Zhang (2014). Ti₃SiC₂ MAX Phase Synthesis by Plasma Basis Method. Universal Journal of Materials Science, 2(5), 83 - 89. DOI: 10.13189/ujms.2014.020501.